电感耦合等离子体发射光谱法测定茶叶籽中多种元素

Determination of elements in tea seeds by inductively coupled plasma atomic emission spectrometry

中文关键词:  电感耦合等离子体发射光谱法  元素  微波消解  茶叶籽

英文关键词:inductively coupled plasma atomic emission spectrometry  elements  microwave digestion  tea seeds

中文摘要:

      目的 对茶叶籽中金属元素进行分析, 为茶叶籽综合利用提供参考。方法 采用高压密闭微波消解结合电感耦合等离子体发射光谱法对茶叶籽中As、Ca、Cd、Cr、Cu、Fe、K、Mg、Mn、Na、Pb、Se及Zn等元素进行了同时快速定量分析。结果 茶叶籽中各元素含量: Mg(1652.23 mg/kg)、Ca(1 026.36 mg/kg)、Mn(122.44 mg/kg)、Na(37.77 mg/kg)、Cr(7.58 mg/kg)、Cu(9.11 mg/kg)、Fe(58.17 mg/kg)、Zn(17.59 mg/kg)、K (9191.29 mg/kg)。As、Cd、Pb及Se未检出。方法加标回收率89%~113%。结论 此方法满足茶叶籽样品中所述元素的分析要求。茶叶籽中钾、镁及钙含量较高, 钠含量相对较低; 锰、铁、锌及铬元素含量丰富。

英文摘要:

      Objective To analyze the etal elements in tea seed, so as to provide a reference for tea seed utilization. Methods Rapid quantitative analysis for elements As, Ca, Cd, Cr, Cu, Fe, K, Mg, Mn, Na, Pb, Se and Zn in tea seeds was carried out by the high-pressure sealed microwave digestion combined with inductively coupled plasma atomic emission spectrometry. Results The content of each element in tea seed were as following: Mg (1652.23 mg/kg), Ca (1 026.36 mg/kg), Mn (122.44 mg/kg), Na (37.77 mg/kg) , Cr (7.58 mg/kg), Cu (9.11 mg/kg), Fe (58.17 mg/kg), Zn (17.59 mg/kg) and K (9191.29 mg/kg), while, As, Cd, Pb and Se were not detected. Method recoveries for all the elements used in this research were between 89% and 113%. Conclusion The method established in this research satisfies the analysis requirements of element in tea seed. Contents of potassium, magnesium and calcium are of high lever in tea seed, while sodium content is relatively low. Tea seed is rich in minor elements such as manganese, iron, zinc and chromium.