于小波,左晓维,李春保.低场核磁共振技术检测猪肉加热终点温度[J].食品安全质量检测学报,2017,8(6):2000-2005
低场核磁共振技术检测猪肉加热终点温度
Detection of endpoint temperature of pork by low field nuclear magnetic resonance
投稿时间:2017-02-28  修订日期:2017-05-09
DOI:
中文关键词:  猪肉  加热终点温度  水分分布  低场核磁共振
英文关键词:pork  endpoint temperature  water distribution  low field nuclear magnetic resonance
基金项目:国家科技支撑计划课题(2012BAD28B02-03, 2014BAD19B01)、国家生猪产业体系(CARS-36-11)、国家重大仪器专项(2013YQ17046308)、中央高校基本科研业务费科技平台实验技术人才基金项目(0806J04)
作者单位
于小波 南京农业大学食品科技学院/教育部肉品加工与质量控制重点实验室 
左晓维 西南大学食品科学学院 
李春保 南京农业大学食品科技学院/教育部肉品加工与质量控制重点实验室 
AuthorInstitution
YU Xiao-Bo College of Food Science and Technology, Nanjing Agricultural University/Key Laboratory of Meat Processing and Quality Control 
ZUO Xiao-Wei College of Food Science, Southwest University 
LI Chun-Bao College of Food Science and Technology, Nanjing Agricultural University/Key Laboratory of Meat Processing and Quality Control 
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中文摘要:
      目的 建立一种基于低场核磁共振技术的猪肉加热终点温度快速检测方法。方法 选择猪背部最长肌于宰后24 h内分别加热至中心温度为40、50、60、70和80 ℃(生肉20 ℃作为对照), 冷却24 h后测定低场核磁共振横向弛豫时间(T2)、蒸煮损失率(cooking loss, CL)。结果 随着加热终点温度升高, 蒸煮损失率显著增加, 低场核磁共振T2谱中第2个峰的峰时间T21和峰面积比P21值差异显著(P<0.05)。因此, T21、P21、CL可作为检测猪肉不同加热终点的指标。结论 研究表明不同加热终点温度的猪肉样品, 低场核磁共振的参数T21、P21以及蒸煮损失的变化有一定规律性, 可用线性回归模型进行预测。该法可用于猪肉加热终点温度的快速检测。
英文摘要:
      Objective To establish a rapid method for determination the endpoint temperature (EPT) of pork by low field nuclear magnetic resonance (LF-NMR). Methods Longissimus dorsi muscles of pork were taken and cooked to a center temperature of 40, 50, 60, 70 and 80 ℃ (the raw sample 20 ℃ as control). The cooked pork was cooled for 24 h and then cooking loss (CL) and low-field nuclear magnetic resonance transverse relaxation time (T2) were measured. Results As cooking EPT increased, CL tended to be increased, and T21 and P21 changed significantly (P<0.05). Therefore, T21, P21 and CL could be used as indicators to detect different EPTs of pork. Conclusion The results show that LF-NMR parameters of T21 and P21 and CL of pork with different EPTs have a certain regularity, which can be predicted by linear regression models. The established method can be used for rapid detection of EPT of pork.
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