| 张媛,丁茹,孙笑笑,李满秀.光化学荧光法测定蔬菜中残留的氯菊酯[J].食品安全质量检测学报,2014,5(3):917-920 |
| 光化学荧光法测定蔬菜中残留的氯菊酯 |
| Study on determination of Propoxur in Vegetable by photochemical-fluorimetry |
| 投稿时间：2014-01-11 修订日期：2014-03-12 |
| DOI： |
| 中文关键词: 氯菊酯 光化学 荧光分析法 |
| 英文关键词:Permethrin photochemistry fluorescence analysis |
| 基金项目:山西省高等学校大学生创新创业训练项目(2012334)、忻州师范学院大学生科技创新项目(2013) |
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| 中文摘要: |
| 在pH 9.29 的B-R缓冲溶液中, 氯菊酯在紫外光照射下发生光化学反应, 其荧光强度明显增强,激发波长为281nm,发射波长为330nm, 由此建立了氯菊酯的光化学-荧光分析法。方法的线性范围为0.004μg/ml---0.036μg/ml, 检出限为0.14ng/mL, 相对标准偏差为1.0%。方法用于蔬菜中氯菊酯残留的测定,结果令人满意。 |
| 英文摘要: |
| A new fluorimetric method based on photochemical reaction for the determination of Propoxur has been developed. It was applied to the determination of Propoxur in vegetables. The method is simple, rapid and easy to operate. The linear relationship between fluorescence intensity and concentration of Propoxur is kept in the range of 0.004μg/ml -0.036μg/ml . The detection limit is 0. 14ng ? mL-1.The method has been applied to the determination of residue propoxur in vegetable with satisfactory results. |
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